

A by UV |
Ratio of absorbance is 1.6 to 1.8 |
1.7 |
B by IR |
IR Conforms to the standard |
Positive |
C by TLC |
Conforms to the standard |
Positive |
Appearance of solution |
Solution should be clear |
Solution is clear |
Absorbance |
At 440nm is not more than 0.1 |
0.02 |
Impurity C |
BY TLC, not more intense than 0.1% |
<0.1% |
Related substances by HPLC |
|
|
Any individual impurity |
Not more than 0.1% |
<0.1% |
Residual solvent |
|
|
Acetone |
Not more than 5000ppm |
Below detection limit |
Methanol |
Not more than 3000ppm |
Below detection limit |
Dichloromethane |
Not more than 100ppm |
Below detection limit |
Acetonitrile |
Not more than 410ppm |
Below detection limit |